FT67 Hydrogenation Unit

 

FT67 Hydrogenation Unit

The Armfield Hydrogenation unit is a floor-standing batch processing vessel, which is used to adjust the degree of saturation of 25 litre batches of edible oils. Increasing the saturation improves the stability and lengthens the shelf-life of the product.

Description

The main processing vessel is situated in a floor-standing stainless steel framework, which also houses a catalyst mixing tank, filter pump, pressure leaf filter and vacuum pump. All equipment in contact with the process fluid is manufactured from stainless steel.

The hydrogenation vessel has a batch capacity of 25 litres.

It is a vertical cylindrical vessel, which incorporates a cooling/steam heating coil, hydrogen gas sparge ring, variable speed turbine agitator and baffle arrangement.

The hydrogen addition cycle results in an exothermic reaction and maintenance of the operating temperature is achieved by circulating metered cooling water through the submerged cooling coil, which removes the excess heat from the reaction. Initial heating to the reaction temperature is by steam, also in the immersed coil. A steam pressure control station enables pressures of up to 10.0 bar on the coil so that process temperatures of up to 180˚C can be achieved. The turbine agitator is driven by a pneumatic motor through a mechanical seal in the lid of the vessel. Rotational speed is varied by adjusting the pressure of the compressed air driving the motor. A maximum speed of 2500 rpm* can be achieved. The propeller mixer in the catalyst preparation tank is also driven by pneumatic motor and is capable of rotating at speeds up to 850 rpm*. Pneumatics are used as the motive force as the presence of hydrogen gas requires minimal use of electrical components. Only the filter charge pump and the liquid ring vacuum pump are driven by electric motor. The centrifugal filter charge pump enables efficient filtering of the catalyst from the oil by the pressure leaf filter, which is a reusable filter requiring no replacement of the filter element. If necessary, filter aid in the form of a diatomaceous earth can be mixed in the catalyst tank and added to the oil charge prior to filtering. The process vessel and filter are designed fully in accordance with the BS 5500 code for pressure vessels. Vacuum levels of 65 mbar are achieved in the reactor vessel by the liquid ring vacuum pump. Reduced system pressures are necessary to prevent oxidation during the heating cycle and assist in the removal of any water present in the oil. Also, the suction pressure is used to charge the vessel with oil and for the addition of catalyst and filter aid.

Technical Specifications

All electrical equipment used on the unit is scheduled flameproof suitable for use in a zone 1 area, which is an area in which an explosive gas air mixture is likely to occur in normal operation. Due to the use of hydrogen gas, the Hydrogenation Unit must be installed in an area designated as safe.

Relevant local regulations regarding the operation of this type of equipment must be adhered to:

Hydrogenation vessel

Total volume: 25 litres

Cooling/heating coil surface area: 0.08m²

Maximum working temperature: 180˚C

Normal working pressure: 0.7bar and 65mbar

Maximum working pressure: 2bar

Agitator drive: pneumatic motor/gearbox

Maximum speed: 2500rpm

Catalyst tank

Volume: 4.0 litres

Stirrer: pneumatic drive, to 850rpm

Filter pump

Type: centrifugal

Impeller: closed

Capacity: 100 l/m @ 2.75 bar

 Liquid ring vacuum pump

Capacity: 66.0m³/hr

Sealant: water

Sealant flow rate: 6.0 l/m

Normal operating pressure: 65mbar

Pressure leaf filter

Material: stainless steel

Filter volume: 3.8 litres

Filter cake capacity: 1.0 litre

Filtering area: 0.09m²

Filter screen: 110 mesh (0.3mm wire)

Maximum pressure: 3.0 bar

Features & Benefits

  • Only 25 litres of oil to be hydrogenated
  • Safe and easy to use
  • Reusable filter mesh
  • Stainless steel pressure vessel
  • Liquid ring vacuum pump
  • Extraction pump
  • Pressure leaf filter
  • Air driven agitators
  • Integral steam heating coil and cooling coil
  • Temperatures to 180˚C
  • Safe zoned controls
  • Accurate control of hydrogen addition
  • Window for safe viewing

Downloads

Heating, Hydrogeneration/Agitation, Cooling.

In order to increase the degree of saturation of edible oils to adjust their physical characteristics, the oil must be mixed with hydrogen gas in the presence of a catalyst under very precisely controlled process conditions. On completion of the reaction, the catalyst must be completely removed by an efficient filtration operation.

The Hydrogenation unit achieves this by use of a variable speed turbine impeller and baffle arrangement, which enables efficient gas/liquid mixing, and accurate control of the pertinent process parameters.

Oil is heated to the desired reaction temperature then hydrogen gas is admitted and fills the vapour space to the pressure required. The progress of the reaction is monitored by regular sample taking and the process stopped when the desired degree of saturation has been obtained.

The Filtration Process

A pressure leaf type filter is used to filter out the catalyst. Due to the small quantities of catalyst involved, a diatomaceous earth is often added to the oil as a filter aid.

This type of filter is the standard used in industry for this duty and provides a convenient method for familiarisation with the operating sequence of such a filter.

Performance

As a guideline to the performance of the hydrogenation unit, typically, using 0.05 – 0.1% active nickel and pure hydrogen, the iodine value (degree of saturation) of cottonseed oil will reduce from 108 to 70 in 40-60 minutes.

The graph indicates the increase in saturation of sunflower oil with time. It was produced from tests carried out by The University of Leeds – Department of Food Science.

Armfield FT67 Hydrogenation Unit

 

 

 

Samples showing the increasing hardness of the oil with process time

  • Electricity supply: Three phase (see ordering codes)
  • Steam supply: 10 kg/hr @ 10 bar min. pressure
  • Compressed air: 25 l/s @ 6 bar min – 10 bar max pressure
  • Cooling Water: 20 l/m @ 3 bar min – 5 bar max pressure
  • Compressed Gas: Hydrogen – 20 l/m @ 2 bar max pressure

Requires an ATEX approved safe working area

Packed and created shipping specifications

Volume: 2.5m³

Gross weight: 500Kg

Length: 1.25m

Width: 0.95m

Height: 1.85m

  • FT67-C: 415V/3ph/50Hz, (6.5kW)
  • FT67-D: 208V/3ph/60Hz, (8.5kW)
  • FT67-E: 380V/3ph/50Hz, (6,5kW)
  • FT67-F: 220V/3ph/60Hz, (8.5kW)
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