FT66 Neutraliser/Washer/Bleacher

 

FT66 Neutraliser/Washer/Bleacher

The Armfield FT66 Neutraliser/Washer/Bleacher is a floor-standing batch processing system. The unit is capable of performing all 3 stages on small quantities of crude edible oils and facilitates practical research and development.

Description

The main reactor vessel, reagent vessels, filter pump and filter are constructed from stainless steel and are mounted within a floor-standing, stainless steel framework. A variable speed agitator, electrical heating element, cooling coil and observation port are incorporated in the reactor, which is a vertical cylindrical vessel designed to process a  25 litre batch of oil.

A liquid ring vacuum pump, also mounted within the framework, is used to create the desired vacuum in the vessel.

Processing under reduced pressure prevents oxidation of the oil and promotes drying. Vacuum suction is also used to charge the reactor  with crude oil and to add reagents and bleaching earth from the appropriate vessels. The reagent tank is used to make up caustic solutions and other additives and to preheat to the desired temperature prior to addition to the reactor. Water for the washing process is also preheated in this vessel. The heating element in the reagent tank is controlled automatically by an electronic controller in the control console. The desired operating temperature of the reactor vessel contents is achieved using an immersed electrical heating element with a maximum power input of 3kW. The heating operation is controlled using a digital display  electronic controller, which automatically maintains the temperature.

Cooling of the hot oil is achieved by circulating cold water through a submerged coil. A flat blade agitator in the reactor is driven by a geared electric motor and the speed of the motor can be adjusted up to a maximum of 1800rpm using a potentiometer on the console.  Agitation of the oil charge promotes mixing of reagents and adsorbents with the oil as well as increasing heat transfer efficiency of the heating and the cooling cycles.

The bleaching earth hopper is a steep sided conical vessel designed  to enable dosing of the required amount of bleaching earth into  the reactor. It is also used for the addition of other adsorbents such as activated carbon. Diatomaceous earth can be charged from this hopper as an aid for the filtering process.

A stainless steel centrifugal pump is used to transfer the oil to  the filter in order to filter out any solids previously added.  The filter is a pressure leaf type, which is designed for repeated use with no consumable filter elements required. By recirculating the oil/ adsorbent mixture through the filter, a layer of solids is built up on the filter mesh screen upon which the remaining solids are deposited. When the oil is clear, it is discharged from the reactor through the filter after which the ‘filter cake’ is dried using compressed air so that it can be removed easily from the filter screen.

Technical Specifications

Reactor vessel

Material: Stainless steel

Total volume: 45 litres

Working volume: 25 litres

Diameter: 0.30m

Height: 0.65m

Heating element: 3.0kW

Cooling coil area: 0.12m²

Agitator speed: 250-1800rpm

Reagent vessel

Material: stainless steel

Working volume: 3 litres

Diameter: 0.165m

Height: 0.20m

Heating element: 1kW

Earth hopper

Material: Stainless steel

Volume: 0.3 litre

Pressure leaf filter

Material: stainless steel

Filter volume: 3.8 litres

Filter cake capacity: 1 litre

Filtering area: 0.09m²

Filter screen: 110 mesh (0.3mm wire)

Maximum pressure: 3.0 bar

Vacuum pump

Type: liquid-ring

Sealant: water

Working vacuum: 75mm Hg (ABS)

Sealant flow rate: 8 l/m

 

Features & Benefits

  • Small quantities of oil can be processed
  • No consumable filter elements required
  • Simple Controls
  • Surfaces in contact with the process fluid are stainless steel
  • Agitation by variable speed flat blade impeller (variable to 1800rpm)
  • Working vacuum of 75mm Hg (ABS) with liquid ring vacuum pump
  • Pressure leaf filter designed to BS5500 – compliant with PED
  • 25 litre vessel designed to BS5500 – compliant with PED
  • Compact and self-contained
  • Cooling coil
  • Extraction pump
  • Electrical heating element

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Crude oil, freshly extracted from seed contains undesirable impurities, which must be removed. These include free fatty acids, phosphatides, colour pigments and fine particles. Using the FT66, the crude oil can be refined by operation in the following modes:

Neutralisation/Washing:

Free fatty acids are removed by neutralising them with a strong base such as caustic soda, which forms a water- soluble soap. The soap is then removed by a combination of thorough washing, gravity settling and draining. Phosphatides are also removed by washing, settling and draining after the addition of phosphoric acid to form water-soluble gums. Any water remaining in the oil is dried by heating the oil under vacuum.

Bleaching:

Colour pigments are removed or reduced by the addition of an adsorbent such as Fullers Earth. The desired colour of the oil can be obtained by adjusting the amount and type of earth used and the physical conditions under which the bleaching operation is carried out.

Filtration:

After bleaching, an efficient filtering process ensures that the earth and other particulates are removed leaving a clean, refined oil ready for further processing such as hardening and deodorising. The filter used for this is a pressure leaf type, which is commonly used in the edible oil industry for the removal of adsorbent.

  • Effect of variation of operating parameters such as temperature, vacuum and degree of agitation
  • Selection of the correct amount and strength of caustic solution for the particular oil
  • Selection of the type and quantity of adsorbent for the bleaching operation
  • Optimisation of operation of a pressure leaf filters
The Armfield FT66 is a floor-standing batch processing vessel capable of carrying out the important pre-refining stages on small quantities of crude edible oils. Suitable for teaching/training and research and development.

  • Electricity supply: Three phase (see ordering codes)
  • Water supply: 30l/m @ 3.0 bar min/5.0 bar max
  • Compressed air: 20l/s @ 3.0 bar min/10.0 bar max

Packed and created shipping specifications

Volume: 2.0m3

Gross weight: 500Kg

Length: 1.28m

Width: 1.90m

Height: 1.90m

  • FT66-C: 415V/3ph/50Hz, (14kW)
  • FT66-D: 208V/3ph/60Hz, (10kW)
  • FT66-E: 380V/3ph/50Hz, (13kW)
  • FT66-F: 220V/3ph/60Hz, (10kW)
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